epr spectrometer modernization

EPR Spectrometer Modernization & Upgrade

Modernize and upgrade your old EPR instrument for cutting-edge EPR research

 

This EPR Modernization and Upgrade service will bring you features including:

Higher Sensitivity: Ultra-low noise microwave source and signal detection technology

Better Resolution: Precise magnetic field control technology

Excellent Compatibility: Compatible with a wide range of EPR spectrometers

Fast Delivery: Complete delivery of the modernized hardware within 2-6 months

High-Quality Service: On-site installation and 2-year warranty

 

★ Email us for more details: info@ciqtek.com

▶ CIQTEK EPR Spectrometer Modernization and Upgrade Pathways

  • CIQTEK EPR Spectrometer Upgrade Pathways

Microwave Bridges

CIQTEK EPR Spectrometer Upgrade -  CW Microwave Bridge Features

CW Microwave Bridge Features

X-band

 • Microwave frequency range: 9.2 to 9.9 GHz
 • Max output microwave power in leveled mode: 200 mW
 • Microwave attenuator: 0 to 60 dB in 1 dB steps
 • Support automated and manual tuning
 • Modernizable to Q-band
 • Size: 85 × 62 × 18 cm

Q-band

 • Microwave frequency: 33.7 to 34.4 GHz
 • Max output microwave power: 100 mW
 • Microwave attenuator: 0 to 50 dB
 • Size: 65 × 62 × 20 cm

CIQTEK EPR Spectrometer Upgrade -  Pulsed microwave amplifier features

Pulsed Microwave Amplifier Features

Solid-state amplifiers have the same linearity and intermodulation distortion as traveling-wave tube amplifiers. Still, they are smaller, have a longer life, and do not require high-voltage power supplies or periodic operation.

X-band

 • Microwave amplifier power: 500 W
 • Size: 43 X 35 X 15 cm

Q-band

 • Solid-state power amplifier power: 200 W
 • Size: 45 × 40 × 16 cm


▶ EPR Spectrometer Console & Magnetic Power Supply

CW Part Features

1. Magnetic Field Controller: Magnetic field stability in sample region: 10 mG/hour; Operating range: -0.1 to 1.8 T

2. Digital Lock-in Detection

3. Ultra Stable Magnet Power Supply

4. Modulation Frequency Range: 0.5 to 120 kHz

 

CIQTEK EPR Spectrometer Upgrade -  Pulsed Part features

Pulsed Part Features

Data Acquisition Unit

 • Number of channels: 2
 • Sampling rate: 1 GHz
 • Supports internal and external trigger modes

Pulse Generator

 • 12 digital channels
 • Time resolution: 0.05 ns

Resonators

▶ High-Q Resonator

1. Cavity resonance frequency: 9.5 to 9.9 GHz

2. Unloaded Q ≥ 16,000 (critically coupled)

3. Maximum modulation field amplitude: 20 Gauss

4. Compatible with the nitrogen and helium variable temperature system

5. Autotune available

CIQTEK EPR Spectrometer Upgrade - High-Q Resonator

Resonator width: 50 mm
Optical window: Ø 5 mm, compatible with optical fiber
Maximum sample access: Ø 10 mm


Dual Mode Resonator

1. Cavity resonance frequency:9.6 to 10 GHz (perpendicular mode), 9.4 to 9.8 GHz (parallel mode)

2. Maximum modulation field amplitude: 10 Gauss

3. Compatible with the nitrogen and helium variable temperature system

CIQTEK EPR Spectrometer Upgrade -  Dual Mode Resonator

Resonator width: 46 mm
Optical window: Ø 5 mm, compatible with optical fiber
Maximum sample access: Ø 10 mm


PW-4201-DR Pulsed Resonator

1. Cavity resonant frequency: 9.4 to 9.8 GHz

2. Resonator bandwidth: 400 ± 40 MHz

3. Detection dead time: ≤ 100 ns

4. Compatible with the nitrogen and helium variable temperature system

CIQTEK EPR Spectrometer Upgrade - PW-4201-DR Pulsed Resonator

Sample rod: 423 mm
Optical window: 5 × 12.5 mm
Flange: KF50
Available sample tube diameter: 3 mm or 4 mm OD


ENDOR Pulsed Resonator

1. Cavity resonant frequency: 9.4 to 9.8 GHz

2. Resonator bandwidth: 400 ± 40 MHz

3. Detection dead time: ≤ 100 ns

4. Compatible with the nitrogen and helium variable temperature system

CIQTEK EPR Spectrometer Upgrade - ENDOR Pulsed Resonator

Sample rod: 423 mm
Optical window: 5 × 12.5 mm
Flange: KF50
Available sample tube diameter: 3 mm or 4 mm OD


Cryogenic Systems

▶ Liquid Helium Continuous-Flow Cryogenics System

CIQTEK EPR Spectrometer Upgrade - Liquid Helium Continuous-Flow Cryogenics System

Controllable Temperature Range (Sample Area): Standard: 4.4–300 K; Optional: 3.2–300 K

Temperature stability: ± 0.1 K (in liquid helium temperature zone)
Rapid cooling: cooling time < 30 minutes
Low liquid helium loss
Easy installation


▶ Liquid Helium-Free Dry Cryogenic System

CIQTEK EPR Spectrometer Upgrade - Liquid Helium-free Dry Cryogenic System

Controllable temperature range of sample area: 4 to 300 K
Temperature stability: ± 0.1 K (in liquid helium temperature zone)
Wider temperature control range
Stable and easy operation
Rapid temperature recovery after sample change (<30 minutes)
Extremely low operating costs

  • CIQTEK EPR Spectrometer Upgrade - CW-type Cryostat
    CW-Type Cryostat

    Compatible with High-Q resonator and Dual-mode resonator.

  • CIQTEK EPR Spectrometer Upgrade - L-type Cryostat
    L-Type Cryostat

    Compatible with the DR pulsed resonator and the ENDOR resonator.
    Cavity ID: 45 mm (wet system); 43 mm (dry system)


Liquid Nitrogen Variable Temperature System

CIQTEK EPR Spectrometer Upgrade - Liquid Nitrogen Variable Temperature System

Controllable temperature range of the sample area: 93 to 573 K
Temperature stability: ± 0.2 K
Rapid cooling: cooling time < 30 minutes
Compatible with high-temperature testing

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